Profile E Strongest 3 peaks no.peak 2Theta d I/I1 FWHM no. (deg) (A) (deg) 1 1 28.3699 3.14332 100 0.11470 2 2 47.2380 1.92256 55 0.10980 56.0600 1.63912 36 0.10770 4000- Peak Data List peak 2Theta d I/I1 FWHM no. (deg) (A) (deg) 1 28.3699 3.14332 100 0.11470 23 47.2380 1.92256 55 0.10980 56.0600 1.63912 36 0.10770 69.0791 1.35858 8 0.11400 76.3222 1.24666 14 0.11000 220 6 87.9814 1.10905 17 0.12150 94.9030 1.04557 8 0.12970 2000 891011 106.6626 0.96033 5 0.15280 114.0568 0.91816 10 0.14960 127.5153 0.85879 8 0.17250 136.8696 0.82826 4 310 0.18340 (400) (33) 51 440 (5311) 620 100 120
(111) (220) (311) (400) (331) (422) (511) (440) (531) (620) (533)
Profile h k 2theta d(A) a(A) 1 1 28.3699 3.14332 5.44439 2 0 47.238 1.92256 5.43782 4000- 2000 12343454565 10 56.06 1.63912 5.43635 69.0791 1.35858 5.43432 3 76.3222 1.24666 5.43406 2 2 87.9814 1.10905 5.43321 1 1 94.903 1.04557 5.43294 4 0 106.6626 0.96033 5.43245 323 114.0568 0.91816 5.43191 0 127.5153 0.85879 5.43146 3 136.8696 0.82826 5.43126 60 100 120
h k l 2theta d(Å) a(Å) 1 1 1 28.3699 3.14332 5.44439 2 2 0 47.238 1.92256 5.43782 3 1 1 56.06 1.63912 5.43635 4 0 0 69.0791 1.35858 5.43432 3 3 1 76.3222 1.24666 5.43406 4 2 2 87.9814 1.10905 5.43321 5 1 1 94.903 1.04557 5.43294 4 4 0 106.6626 0.96033 5.43245 5 3 1 114.0568 0.91816 5.43191 6 2 0 127.5153 0.85879 5.43146 5 3 3 136.8696 0.82826 5.43126
误差来源 1.0 △sin0 0.8 ① 0.6 △0→ 0.4- 元 d 0.2- 2sin0 0.0 0 20 40 60 80 0(degrees)
误差来源 2sin d
误差来源 λ d 2sin0 △几 λ△0cos0 △d= 2sin0 2sin2 0 △d △几 △θcos0 d λ sinθ
误差来源 2 2sin cos 2sin d 2sin d sin cos d d